Petrochemical Inductively CoupledPlasma Optical Emission Spectrometer（ICP6800S） is aprofessional instrument for the petrochemical industry launched by MacylabInstruments. It can be used to determine more than 30 elements in crude oil,mainly for Fe.Na.Mg.Ni. V.Ca. Pb.Mo.Mn.Cr.Ca.Ba.As; also can be used to measureiron, manganese, lead, silicon in gasoline ,ａnd the Wear elements of additivein lubricating oil, it also can be applied for multielement determination inbase oils; for the determination of sodium in formaldehyde and thedetermination of oil field tracer.

Application Environment

CONTENT RANGE

Shipping/StorageAmbient Temperature 15℃-25℃

Shipping/StorageRelative Humidity ≤70％

Atmosphericpressure 86-106 kPa

PowerSupply 220±10V 50-60MHz

WorkingHumidity ≤70％

WorkingTemperature 15℃-30℃

Technical Parameter

RFPower technical parameter：

Circuittype: solid-state RF power supply, with function of automatch

Frequency:27.12MHz±0.05％

FrequencyStability: ＜0.1%

PowerOutput: 800W—1500W

PowerOutput Stability: ＜0.3%

EscapedRF radiation: 30cm away from the instrument, electric field: E﹤2V/m

Sampling System Technical Parameter：

Outputworking coil inner diameter ：25mm

Torquetube: Three concentric, external diameter 20mm

Coaxialnebulizer:Outer diameter 6mm

Doublebarrel atomizing chamber: Outer diameter 34mm

Gas Flow Controls

1.Plasma Argon Flowmeter:（100-1000）L/h (1.6-16L/min)

2.Auxiliary Argon Flowmeter:（10-100）L/h (0.16-1.66L/min)

3.Carrier Argon Flowmeter（10-100）L/h (0.16-1.66L/min)

4.OxygenFlowmeter:（0-100）ml/min (30-50ml/min)

5.PressureMaintaining Valve（0-0.4MPa）

6.CoolingWater：Temperature: 20-25℃, Rate of Flow>5L/min, Hydraulic Pressure>0.1MPa

Spectrometer

Optics：Czerny-Turnertype

Focallength: 1000 mm

Grating:Ion Beam Etching Holographic Grating, 4320L/mm

Reciprocallinear dispersion: 0.26nm/mm

Resolution:≤ 0.005nm(4320 line grating)

Wavelengthrange: 4320 line grating:(180nm～435) nm

Minimumpace of stepping motor: ≤0.0006 nm

ExitSlit:10μm；Entrance Slit:8μm

Photoelectric Converter Performance

Photomultipliertube specification: R293

NegativeHV on PMT: 0-1000V;Stability: ＜0.05%

Refrigeration System

RefrigeratingSwirling Fog Chamber：The use of imported silica gel collection technology can make thetemperature drop to 20 degrees below zero

Overall Performance

Wavelengthrange of scanning: 185nm～435nm(4320L/mm line grating)

Repeatability:RSD(Relative Standard Deviation)≤1.5％

Stability:RSD(Relative Standard Deviation) ≤2％

DetectionLimits (µg/L):

Directinjection sampling and measure iron(Fe), manganese(Mn), lead(Pb) andsilicon(Si) in gasoline.Analysis results:

Element	Fe	Mn	Pb	Si
Determination value/(mg/L)	3.6	17.5	1.8	2.4
RSD/%	0.56	0.23	1.38	0.92

StandardAdditionａnd Recovery Rate:

Number	Standard Addition （mg/L）	Fe		Mn		Pb			Si
		Determination value（mg/L）	Recovery /%	Determination value（mg/L）	Recovery /%	Determination value（mg/L）	Recovery /%	Determination value（mg/L）		Recovery /%
1	0.45	0.436	96.9	0.468	104.0	0.432	96.0	0.465		103.3
2	0.9	0.887	98.6	0.913	101.4	0.868	96.4	0.919		102.1

　　Macy(China) Instruments Inc is part of Shanghai Macylab Instrument Inc, is a high-tech enterprise with independent intellectual property rights . Macy hold the pioneering concept "technology - because you change " , and as a business purpose, and constantly explore, bold innovation. Especially in the field of analytical instruments ,Macy constantly develop advanced products that enable Macy to become a high-quality instrument resource supplier and leader。